Microwave and Ultrasonic Pretreatment-Assisted Upgradation of Iron Ore of Karnataka Region from India
DOI:
https://doi.org/10.18311/jmmf/2023/33576Keywords:
Grinding Energy, Iron Ore, Microwave, Ultrasonication, Work IndexAbstract
Essentially, size reduction is the very first and vital segment of mineral processing. Microwaves (MW) for comminution have piqued the interest of researchers and industrialists in recent years. The use of microwaves in processing industries is solely due to some of the unique benefits they provide. Because MW heating does not rely on temperature gradients but instead generates heat as a result of molecules interacting with microwaves and the resulting internal friction, this treatment can result in rapid and volumetric heating. Because of these factors, this treatment can significantly reduce process times while also improving product quality. The current study demonstrated the formation of intergranular fractures and their influence on comminution energy after MW treatment of Indian iron ore. Scanning Electron Microscopy (SEM) analysis confirmed that pretreatment with MW made the ore more brittle, making it more amenable to grinding, and a decrease in grinding energy of the pretreated ore was observed in comparison to the untreated sample. The X-Ray Diffraction (XRD) results demonstrated an increase in ore crystallinity following MW exposure, substantiating the pretreated sample's lower grinding energy consumption. Additionally, ultrasonication of MW pretreated ore was attempted to determine whether the combined treatment method could improve the ore quality, and the combination techniques were successful in increasing the iron content by 41% while decreasing the alumina and silica contents by 59% and 38%, respectively. The findings support the use of both MW irradiation and ultrasonication as promising methods of improving mineral quality.
Downloads
Metrics
Downloads
Published
How to Cite
Issue
Section
License
This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.
Accepted 2023-11-15
Published 2023-11-15
References
Wills BA. An introduction to the practical aspects of ore treatment and mineral recovery. Mineral Processing Technology - Oxford. Elsevier; 2006.
Joseph K. Microwave enhanced processing of ores [PhD thesis] UK: The University of Nottingham; 2010.
Wills BA. Mineral processing technology: An introduction to the practical aspects of ore treatment and mineral recovery. 6th ed. Oxford, England: Butterworth- Heinemann; 1997.
Napier-Munn TJ. Mineral communication circuits - Their operation and optimization. Julius Kruttschnitt Mineral Research Center; 1999.
Wills BA, Atkinson K. Some observations on the fracture and liberation of mineral assemblies. Miner Eng [Internet]. 1993; 6(7):697–706. https://doi. org/10.1016/0892-6875(93)90001-4
Kingman SW. The influence of microwave radiation on the comminution and beneficiation of minerals. UK: University of Birmingham; 1999.
Jones DA, Kingman SW, Whittles DN, Lowndes IS. The influence of microwave energy delivery method on strength reduction in ore samples. Chem Eng Process [Internet]. 2007; 46(4):291–9. https://doi.org/10.1016/j. cep.2006.06.009
Siores E, Do Rego D. Microwave applications in materials joining. J Mater Process Technol [Internet]. 1995; 48(1–4):619–25. https://doi.org/10.1016/0924- 0136(94)01701-2
Standish N, Huang W. Microwave application in carbothermic reduction of iron ores. ISIJ Int [Internet]. 1991; 31(3):241–5. https://doi.org/10.2355/ isijinternational.31.241
Woodcock JT. Possibilities for use of microwave radiation in the processing of gold. In: Proc First Aus Symp on Microwave Power Applications. 1989; 139-42.
Zavitsonas PD. Coal desulphurization using microwave radiation. US Patent. Patent No: DOE.PC 30142-71; 1981.
Butcher DA, Rowson NA. Microwave desulphurization of coal. I Chem E Research Event. 1995; 1:583–5.
Rowson NA, Rice NM. Desulphurization of coal using low-power microwave energy. Minerals Engineering. 1990; 3:364–8. https://doi.org/10.1016/0892- 6875(90)90131-T
Vorster W, Rowson NA, Kingman SW. The effect of microwave radiation upon the processing of Neves Corvo copper ore. Int J Miner Process [Internet]. 2001; 63(1):29–44. https://doi.org/10.1016/S0301-7516(00)00069-7
Rayapudi V, Agrawal S, Dhawan N. Investigation of microwave exposure on beneficiation of low-grade banded iron ore. Min Metall Explor [Internet]. 2019; 36(2):327–34. https://doi.org/10.1007/s42461-018- 0017-7
Vorster W. The effect of microwave radiation on mineral processing. The University of Birmingham; 2001. https:// doi.org/10.1016/S0301-7516(00)00069-7
Donskoi E, Collings AF, Poliakov A, Bruckard WJ. Utilization of ultrasonic treatment for upgrading of hematitic/goethitic iron ore fines. Int J Miner Process [Internet]. 2012; 114–117:80–92. https://doi. org/10.1016/j.minpro.2012.10.005
Pandey JC, Sinha M, Raj M. Reducing alumina, silica and phosphorus in iron ore by high-intensity power ultrasound. Ironmaking and Steelmaking. 2013; 37(8):583–9. https://doi.org/10.1179/0301923 10X12731438632083
Zhang Y, Jie J, Gao Y, Lu Y, Li T. Effects of ultrasonic treatment on the formation of iron-containing intermetallic compounds in Al-12% Si-2% Fe alloys. Intermetallics (Barking) [Internet]. 2013; 42:120–5. https://doi.org/10.1016/j.intermet.2013.05.018
Omran M, Fabritius T, Abdel-Khalek N, El-Aref M, Elmanawi AE-H, Nasr M, et al. Microwave-assisted liberation of high phosphorus Oolitic iron ore. J Miner Mater Charact Eng [Internet]. 2014; 02(05):414–27. https://doi.org/10.4236/jmmce.2014.25046
Omran M, Fabritius T, Elmahdy AM, Abdel-Khalek NA, El-Aref M, Elmanawi AE-H. Effect of microwave pretreatment on the magnetic properties of iron ore and its implications on magnetic separation. Sep Purif Technol [Internet]. 2014; 136:223–32. https://doi.org/10.1016/j. seppur.2014.09.011
Omran M, Fabritius T, Elmahdy AM, Abdel-Khalek NA, El-Aref M, Elmanawi AE-H. XPS and FTIR spectroscopic study on microwave-treated high phosphorus iron ore. Applied Surface Science. 2015; 345:127-40. https://doi. org/10.1016/j.apsusc.2015.03.209
Jones DA, Kingman SW, Whittles DN, Lowndes IS. Understanding microwave-assisted breakage. Miner Eng [Internet]. 2005; 18(7):659–69. https://doi.org/10.1016/j. mineng.2004.10.011
Sahoo BK, De S, Meikap BC. Improvement of grinding characteristics of Indian coal by microwave pre-treatment. Fuel Process Technol [Internet]. 2011; 92(10):1920–8. https://doi.org/10.1016/j. fuproc.2011.05.012
Song S, Campos-Toro EF, López-Valdivieso A. Formation of micro-fractures on an oolitic iron ore under microwave treatment and its effect on selective fragmentation. Powder Technol [Internet]. 2013; 243:155–60. https:// doi.org/10.1016/j.powtec.2013.03.049
Amankwah RK, Khan AU, Pickles CA, Yen WT. Improved grindability and gold liberation by microwave pretreatment of free-milling gold ore. Miner Process Extr Metall [Internet]. 2005; 114(1):30–6. https://doi. org/10.1179/037195505X28447
Ebadnejad A. Investigating the effect of rework index and particle size on the grinding modeling of some copper sulfide ores. Journal of Materials Research and Technology. 2016; 5(2):101–10. https://doi. org/10.1016/j.jmrt.2015.05.002
Olatunji KJ, Durojaiye AG. Determination of bond index of Birnin-Gwari iron ore in Nigeria. Journal of Minerals and Materials Characterization and Engineering. 2010; 9(7):635–42. https://doi.org/10.4236/jmmce.2010.97045
Magdalinović NM. Calculation of energy required for grinding in a ball mill. Int J Miner Process [Internet]. 1989; 25(1–2):41–6. https://doi.org/10.1016/0301- 7516(89)90055-0
Scott G, Bradshaw SM, Eksteen JJ. The effect of microwave pretreatment on the liberation of a copper carbonite ore after milling. International Journal of Mineral Processing. 2008; 85:121–8. https://doi. org/10.1016/j.minpro.2007.08.005
Samanli S. A comparison of the results obtained from grinding in a stirred media mill lignite coal samples treated with microwave and untreated samples. Fuel. 2011; 90:659–64. https://doi.org/10.1016/j. fuel.2010.10.014
Koleini J, Barani SM, Rezaei K. microwave treatment on dry grinding kinetics of iron ore. Mineral Processing and Extractive Metallurgy Review. An International Journal. 2012; 33(3):159–69. https://doi.org/10.1080/08 827508.2011.562947
Omran M, Fabritius T, Mattila R. Thermally assisted liberation of high phosphorus oolitic iron ore: A comparison between microwave and conventional furnaces. Powder Technology. 2015; 269:7–14. https:// doi.org/10.1016/j.powtec.2014.08.073
Rizmanoski V. The effect of microwave pretreatment on impact breakage of copper ore. Miner Eng [Internet]. 2011; 24(14):1609–18. https://doi.org/10.1016/j. mineng.2011.08.017